<?xml version="1.0" encoding="utf-8"?>
<TEI xmlns="http://www.tei-c.org/ns/1.0" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns:hal="http://hal.archives-ouvertes.fr/" xmlns:gml="http://www.opengis.net/gml/3.3/" xmlns:gmlce="http://www.opengis.net/gml/3.3/ce" version="1.1" xsi:schemaLocation="http://www.tei-c.org/ns/1.0 http://api.archives-ouvertes.fr/documents/aofr-sword.xsd">
  <teiHeader>
    <fileDesc>
      <titleStmt>
        <title>HAL TEI export of hal-04780151</title>
      </titleStmt>
      <publicationStmt>
        <distributor>CCSD</distributor>
        <availability status="restricted">
          <licence target="https://creativecommons.org/publicdomain/zero/1.0/">CC0 1.0 - Universal</licence>
        </availability>
        <date when="2026-05-25T03:53:54+02:00"/>
      </publicationStmt>
      <sourceDesc>
        <p part="N">HAL API Platform</p>
      </sourceDesc>
    </fileDesc>
  </teiHeader>
  <text>
    <body>
      <listBibl>
        <biblFull>
          <titleStmt>
            <title xml:lang="en">Monitoring of Ammonium and Nitrate Ions in Soil Using Ion-Sensitive Potentiometric Microsensors</title>
            <author role="aut">
              <persName>
                <forename type="first">Matthieu</forename>
                <surname>Joly</surname>
              </persName>
              <idno type="halauthorid">1300264-0</idno>
              <affiliation ref="#struct-392533"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Maurane</forename>
                <surname>Marlet</surname>
              </persName>
              <idno type="halauthorid">1315503-0</idno>
              <affiliation ref="#struct-574390"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">David</forename>
                <surname>Barreau</surname>
              </persName>
              <idno type="halauthorid">2386475-0</idno>
              <affiliation ref="#struct-1214268"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Arnaud</forename>
                <surname>Jourdan</surname>
              </persName>
              <idno type="halauthorid">1352989-0</idno>
              <affiliation ref="#struct-1214268"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Céline</forename>
                <surname>Durieu</surname>
              </persName>
              <idno type="halauthorid">1315504-0</idno>
              <affiliation ref="#struct-574390"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Jérôme</forename>
                <surname>Launay</surname>
              </persName>
              <email type="md5">6c2aa36d149518d71d2c5565e35aa41c</email>
              <email type="domain">laas.fr</email>
              <idno type="idhal" notation="string">jerome-launay</idno>
              <idno type="idhal" notation="numeric">1005707</idno>
              <idno type="halauthorid" notation="string">1157856-1005707</idno>
              <idno type="IDREF">https://www.idref.fr/070840520</idno>
              <affiliation ref="#struct-392533"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Pierre</forename>
                <surname>Temple-Boyer</surname>
              </persName>
              <email type="md5">c4aa31fa03b35faf1ae38ebc29ba3e70</email>
              <email type="domain">laas.fr</email>
              <idno type="idhal" notation="string">pierre-temple-boyer</idno>
              <idno type="idhal" notation="numeric">4211</idno>
              <idno type="halauthorid" notation="string">18237-4211</idno>
              <idno type="IDREF">https://www.idref.fr/082101469</idno>
              <affiliation ref="#struct-392533"/>
            </author>
            <editor role="depositor">
              <persName>
                <forename>Pierre</forename>
                <surname>Temple-Boyer</surname>
              </persName>
              <email type="md5">c4aa31fa03b35faf1ae38ebc29ba3e70</email>
              <email type="domain">laas.fr</email>
            </editor>
            <funder>Fonds unique interministériel et Région "Midi-Pyrénées" (projet FUI AAP 16, n°F1401015M)</funder>
          </titleStmt>
          <editionStmt>
            <edition n="v1" type="current">
              <date type="whenSubmitted">2024-11-13 12:32:18</date>
              <date type="whenWritten">2024-10-25</date>
              <date type="whenModified">2025-10-22 18:04:09</date>
              <date type="whenReleased">2024-11-18 16:22:50</date>
              <date type="whenProduced">2024-11-06</date>
              <date type="whenEndEmbargoed">2024-11-13</date>
              <ref type="file" target="https://laas.hal.science/hal-04780151v1/document">
                <date notBefore="2024-11-13"/>
              </ref>
              <ref type="file" subtype="author" n="1" target="https://laas.hal.science/hal-04780151v1/file/manuscript_ISFET_for_soil_analysis_vf.pdf" id="file-4780151-4162384">
                <date notBefore="2024-11-13"/>
              </ref>
            </edition>
            <respStmt>
              <resp>contributor</resp>
              <name key="316686">
                <persName>
                  <forename>Pierre</forename>
                  <surname>Temple-Boyer</surname>
                </persName>
                <email type="md5">c4aa31fa03b35faf1ae38ebc29ba3e70</email>
                <email type="domain">laas.fr</email>
              </name>
            </respStmt>
          </editionStmt>
          <publicationStmt>
            <distributor>CCSD</distributor>
            <idno type="halId">hal-04780151</idno>
            <idno type="halUri">https://laas.hal.science/hal-04780151</idno>
            <idno type="halBibtex">joly:hal-04780151</idno>
            <idno type="halRefHtml">&lt;i&gt;Sensors&lt;/i&gt;, 2024, 24 (22), pp.7143. &lt;a target="_blank" href="https://dx.doi.org/10.3390/s24227143"&gt;&amp;#x27E8;10.3390/s24227143&amp;#x27E9;&lt;/a&gt;</idno>
            <idno type="halRef">Sensors, 2024, 24 (22), pp.7143. &amp;#x27E8;10.3390/s24227143&amp;#x27E9;</idno>
            <availability status="restricted">
              <licence target="https://about.hal.science/hal-authorisation-v1/">HAL Authorization<ref corresp="#file-4780151-4162384"/></licence>
            </availability>
          </publicationStmt>
          <seriesStmt>
            <idno type="stamp" n="UNIV-TLSE2">Université Toulouse 2</idno>
            <idno type="stamp" n="UNIV-TLSE3">Université de Toulouse</idno>
            <idno type="stamp" n="CNRS">CNRS - Centre national de la recherche scientifique</idno>
            <idno type="stamp" n="INSA-TOULOUSE">Institut National des Sciences Appliquées de Toulouse</idno>
            <idno type="stamp" n="LAAS">Laboratoire d'analyse et d'architecture des systèmes</idno>
            <idno type="stamp" n="UT1-CAPITOLE">Université Toulouse 1 Capitole</idno>
            <idno type="stamp" n="LAAS-MICA">Equipe MICrosystèmes d'Analyse</idno>
            <idno type="stamp" n="LAAS-MICRO-NANO-BIO-TECHNOLOGIES" corresp="LAAS">LAAS-Micro Nano Bio Technologies</idno>
            <idno type="stamp" n="INSA-GROUPE">Groupe INSA</idno>
            <idno type="stamp" n="TOULOUSE-INP">Toulouse - INP</idno>
            <idno type="stamp" n="UNIV-UT3">Université Toulouse 3</idno>
            <idno type="stamp" n="UT3-INP">Université de Toulouse / Toulouse INP</idno>
            <idno type="stamp" n="UT3-TOULOUSEINP">Université de Toulouse / Toulouse INP</idno>
            <idno type="stamp" n="TEST7-HALCNRS">test 7 du portail hal cnrs</idno>
            <idno type="stamp" n="RENATECH">RENATECH</idno>
          </seriesStmt>
          <notesStmt>
            <note type="audience" n="2">International</note>
            <note type="invited" n="0">No</note>
            <note type="popular" n="0">No</note>
            <note type="peer" n="1">Yes</note>
          </notesStmt>
          <sourceDesc>
            <biblStruct>
              <analytic>
                <title xml:lang="en">Monitoring of Ammonium and Nitrate Ions in Soil Using Ion-Sensitive Potentiometric Microsensors</title>
                <author role="aut">
                  <persName>
                    <forename type="first">Matthieu</forename>
                    <surname>Joly</surname>
                  </persName>
                  <idno type="halauthorid">1300264-0</idno>
                  <affiliation ref="#struct-392533"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Maurane</forename>
                    <surname>Marlet</surname>
                  </persName>
                  <idno type="halauthorid">1315503-0</idno>
                  <affiliation ref="#struct-574390"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">David</forename>
                    <surname>Barreau</surname>
                  </persName>
                  <idno type="halauthorid">2386475-0</idno>
                  <affiliation ref="#struct-1214268"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Arnaud</forename>
                    <surname>Jourdan</surname>
                  </persName>
                  <idno type="halauthorid">1352989-0</idno>
                  <affiliation ref="#struct-1214268"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Céline</forename>
                    <surname>Durieu</surname>
                  </persName>
                  <idno type="halauthorid">1315504-0</idno>
                  <affiliation ref="#struct-574390"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Jérôme</forename>
                    <surname>Launay</surname>
                  </persName>
                  <email type="md5">6c2aa36d149518d71d2c5565e35aa41c</email>
                  <email type="domain">laas.fr</email>
                  <idno type="idhal" notation="string">jerome-launay</idno>
                  <idno type="idhal" notation="numeric">1005707</idno>
                  <idno type="halauthorid" notation="string">1157856-1005707</idno>
                  <idno type="IDREF">https://www.idref.fr/070840520</idno>
                  <affiliation ref="#struct-392533"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Pierre</forename>
                    <surname>Temple-Boyer</surname>
                  </persName>
                  <email type="md5">c4aa31fa03b35faf1ae38ebc29ba3e70</email>
                  <email type="domain">laas.fr</email>
                  <idno type="idhal" notation="string">pierre-temple-boyer</idno>
                  <idno type="idhal" notation="numeric">4211</idno>
                  <idno type="halauthorid" notation="string">18237-4211</idno>
                  <idno type="IDREF">https://www.idref.fr/082101469</idno>
                  <affiliation ref="#struct-392533"/>
                </author>
              </analytic>
              <monogr>
                <idno type="localRef">Rapport LAAS n° 24475</idno>
                <idno type="halJournalId" status="VALID">55556</idno>
                <idno type="issn">1424-8220</idno>
                <title level="j">Sensors</title>
                <imprint>
                  <publisher>MDPI</publisher>
                  <biblScope unit="volume">24</biblScope>
                  <biblScope unit="issue">22</biblScope>
                  <biblScope unit="pp">7143</biblScope>
                  <date type="datePub">2024-11-06</date>
                  <date type="dateEpub">2024-11-06</date>
                </imprint>
              </monogr>
              <idno type="doi">10.3390/s24227143</idno>
              <ref type="publisher">https://www.mdpi.com/1424-8220/24/22/7143</ref>
            </biblStruct>
          </sourceDesc>
          <profileDesc>
            <langUsage>
              <language ident="en">English</language>
            </langUsage>
            <textClass>
              <keywords scheme="author">
                <term xml:lang="en">ammonium NH 4 + ion</term>
                <term xml:lang="en">ion-sensitive layers</term>
                <term xml:lang="en">soil analysis</term>
                <term xml:lang="en">nitrate NO 3 -ion</term>
                <term xml:lang="en">potentiometric sensor</term>
                <term xml:lang="en">ISFET</term>
                <term xml:lang="en">ion-sensitive field effect transistor</term>
              </keywords>
              <classCode scheme="halDomain" n="spi">Engineering Sciences [physics]</classCode>
              <classCode scheme="halTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halOldTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halTreeTypology" n="ART">Journal articles</classCode>
            </textClass>
            <abstract xml:lang="en">
              <p>Focusing on the ChemFET (chemical field-effect transistor) technology, the development of a multi-microsensor platform for soil analysis is described in this work. Thus, different FET-based microdevices (i.e., pH-ChemFET pNH4-ISFET and pNO3-ISFET sensors) were realized with the aim of monitoring nitrogen-based ionic species in soil, evidencing quasi-Nernstian detection properties (&amp;gt;50 mV/decade) in appropriate concentration ranges for agricultural applications. Using a specific test bench adapted to important earth samples (mass: ~50 kg), first experiments were done in a lab, mimicking rainy periods as well as nitrogen-based fertilizer inputs. By monitoring pH, pNH4, and pNO3 in an acidic (pH ≈ 4.7) clay-silt soil matrix, different processes associated to the nitrogen cycle were characterized over a fortnight, demonstrating comprehensive results for ammonium nitrate NH4NO3 inputs at different concentrations, water additions, nitrification phenomena, and ammonium NH4+ ion trapping. Even if the ChemFET-based measurement system should be improved according to the soil(electrolyte)/sensor contact, such realizations and results show the ChemFET technology potentials for long-term analysis in soil, paving the way for future “in situ” approaches in the frame of modern farming.</p>
            </abstract>
            <particDesc>
              <org type="ir" xml:id="fr-esr-fdr-ir-097">
                <orgName type="acronym">RENATECH+</orgName>
                <idno type="wikidata">Q33121910</idno>
              </org>
            </particDesc>
          </profileDesc>
        </biblFull>
      </listBibl>
    </body>
    <back>
      <listOrg type="structures">
        <org type="researchteam" xml:id="struct-392533" status="OLD">
          <orgName>Équipe MICrosystèmes d'Analyse</orgName>
          <orgName type="acronym">LAAS-MICA</orgName>
          <date type="end">2025-01-01</date>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.laas.fr/public/fr/mica</ref>
          </desc>
          <listRelation>
            <relation active="#struct-459" type="direct"/>
            <relation active="#struct-81148" type="indirect"/>
            <relation name="443875" active="#struct-443875" type="indirect"/>
            <relation active="#struct-116255" type="indirect"/>
            <relation active="#struct-301232" type="indirect"/>
            <relation active="#struct-443875" type="indirect"/>
            <relation active="#struct-116256" type="indirect"/>
            <relation active="#struct-217752" type="indirect"/>
            <relation name="UPR8001" active="#struct-441569" type="indirect"/>
            <relation active="#struct-448187" type="indirect"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-574390" status="VALID">
          <orgName>Agronutrition</orgName>
          <desc>
            <address>
              <addrLine>Parc Activestre - 3 avenue de l'orchidée31390 CARBONNE</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.agronutrition.com/fr</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-1214268" status="INCOMING">
          <orgName>SIREA SA</orgName>
          <desc>
            <address>
              <country key="FR"/>
            </address>
          </desc>
        </org>
        <org type="laboratory" xml:id="struct-459" status="OLD">
          <idno type="IdRef">199278792</idno>
          <idno type="ISNI">0000 0001 2188 216X </idno>
          <idno type="RNSR">199517454Y</idno>
          <idno type="ROR">https://ror.org/03vcm6439</idno>
          <orgName>Laboratoire d'analyse et d'architecture des systèmes</orgName>
          <orgName type="acronym">LAAS</orgName>
          <date type="start">1968-01-01</date>
          <date type="end">2025-01-01</date>
          <desc>
            <address>
              <addrLine>7 Av du colonel Roche 31077 TOULOUSE CEDEX 4</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.laas.fr</ref>
          </desc>
          <listRelation>
            <relation active="#struct-81148" type="direct"/>
            <relation name="443875" active="#struct-443875" type="indirect"/>
            <relation active="#struct-116255" type="direct"/>
            <relation active="#struct-301232" type="indirect"/>
            <relation active="#struct-443875" type="indirect"/>
            <relation active="#struct-116256" type="direct"/>
            <relation active="#struct-217752" type="direct"/>
            <relation name="UPR8001" active="#struct-441569" type="direct"/>
            <relation active="#struct-448187" type="direct"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-81148" status="VALID">
          <idno type="IdRef">026404354</idno>
          <idno type="ISNI">0000000121902837</idno>
          <idno type="ROR">https://ror.org/0443n9e75</idno>
          <orgName>Université Toulouse Capitole</orgName>
          <orgName type="acronym">UT Capitole</orgName>
          <date type="start">1970-01-01</date>
          <desc>
            <address>
              <addrLine>2 rue du Doyen-Gabriel-Marty - 31042 Toulouse Cedex 9</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.ut-capitole.fr/</ref>
          </desc>
          <listRelation>
            <relation name="443875" active="#struct-443875" type="direct"/>
          </listRelation>
        </org>
        <org type="regroupinstitution" xml:id="struct-443875" status="VALID">
          <idno type="ROR">https://ror.org/017tgbk05</idno>
          <orgName>Communauté d'universités et établissements de Toulouse</orgName>
          <orgName type="acronym">Comue de Toulouse</orgName>
          <desc>
            <address>
              <addrLine>41 Allée Jules Guesde, 31000 Toulouse</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.univ-toulouse.fr/</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-116255" status="VALID">
          <idno type="IdRef">026388766</idno>
          <idno type="ISNI">0000 0001 2286 8343</idno>
          <idno type="ROR">https://ror.org/01h8pf755</idno>
          <idno type="Wikidata">Q858979</idno>
          <orgName>Institut National des Sciences Appliquées - Toulouse</orgName>
          <orgName type="acronym">INSA Toulouse</orgName>
          <date type="start">1963-10-21</date>
          <desc>
            <address>
              <addrLine>135, avenue de Rangueil - 31077 Toulouse cedex 4</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.insa-toulouse.fr</ref>
          </desc>
          <listRelation>
            <relation active="#struct-301232" type="direct"/>
            <relation active="#struct-443875" type="direct"/>
          </listRelation>
        </org>
        <org type="regroupinstitution" xml:id="struct-301232" status="VALID">
          <idno type="IdRef">162105150</idno>
          <orgName>Institut National des Sciences Appliquées</orgName>
          <orgName type="acronym">INSA</orgName>
          <desc>
            <address>
              <country key="FR"/>
            </address>
          </desc>
        </org>
        <org type="institution" xml:id="struct-116256" status="VALID">
          <idno type="IdRef">026403994</idno>
          <idno type="ROR">https://ror.org/04ezk3x31</idno>
          <orgName>Université Toulouse - Jean Jaurès</orgName>
          <orgName type="acronym">UT2J</orgName>
          <date type="start">1971-01-01</date>
          <desc>
            <address>
              <addrLine>5 allées Antonio Machado - 31058 Toulouse Cedex 9</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.univ-tlse2.fr</ref>
          </desc>
          <listRelation>
            <relation active="#struct-443875" type="direct"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-217752" status="OLD">
          <idno type="IdRef">026404672</idno>
          <idno type="ISNI">0000000121617331</idno>
          <idno type="ROR">https://ror.org/02v6kpv12</idno>
          <idno type="Wikidata">Q1273188</idno>
          <orgName>Université Toulouse III - Paul Sabatier</orgName>
          <orgName type="acronym">UT3</orgName>
          <date type="end">2025-01-01</date>
          <desc>
            <address>
              <addrLine>118 route de Narbonne - 31062 Toulouse</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.univ-tlse3.fr/</ref>
          </desc>
          <listRelation>
            <relation active="#struct-443875" type="direct"/>
          </listRelation>
        </org>
        <org type="regroupinstitution" xml:id="struct-441569" status="VALID">
          <idno type="IdRef">02636817X</idno>
          <idno type="ISNI">0000000122597504</idno>
          <idno type="ROR">https://ror.org/02feahw73</idno>
          <orgName>Centre National de la Recherche Scientifique</orgName>
          <orgName type="acronym">CNRS</orgName>
          <date type="start">1939-10-19</date>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.cnrs.fr/</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-448187" status="VALID">
          <idno type="IdRef">026388820</idno>
          <idno type="ISNI">0000000121766169</idno>
          <idno type="ROR">https://ror.org/033p9g875</idno>
          <orgName>Institut National Polytechnique (Toulouse)</orgName>
          <orgName type="acronym">Toulouse INP</orgName>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.inp-toulouse.fr/</ref>
          </desc>
          <listRelation>
            <relation active="#struct-443875" type="direct"/>
          </listRelation>
        </org>
      </listOrg>
    </back>
  </text>
</TEI>